Isingeniso se-Small Peptide Trace Mineral Chelates
Ingxenye 1 Umlando Wokulandelela Izithako Zamaminerali
Ingahlukaniswa izizukulwane ezine ngokusho kokuthuthukiswa kwezithasiselo zamaminerali:
Isizukulwane sokuqala: Usawoti we-Inorganic of trace minerals, njenge-copper sulfate, i-ferrous sulfate, i-zinc oxide, njll; Isizukulwane sesibili: Usawoti we-Organic acid wamaminerali okulandelela, njenge-ferrous lactate, i-ferrous fumarate, i-copper citrate, njll.; Isizukulwane sesithathu: I-amino acid chelate feed grade of trace minerals, njenge-zinc methionine, iron glycine kanye ne-zinc glycine; Isizukulwane sesine: Amaprotheni nosawoti kanye ne-peptide chelating usawoti wamaminerali amancane, njenge-protein yethusi, i-protein iron, i-protein zinc, i-protein manganese, ithusi elincane le-peptide, i-peptide iron encane, i-peptide zinc encane, i-peptide manganese encane, njll.
Isizukulwane sokuqala amaminerali e-inorganic trace, kanti isizukulwane sesibili kuya kwesesine amaminerali e-organic trace.
Ingxenye 2 Kungani Khetha Ama-Peptide Chelates Amancane
Ama-peptide chelates amancane anokusebenza okulandelayo:
1. Lapho ama-peptide amancane e-chelate nama-ion ensimbi, acebile ngamafomu futhi anzima ukugcwaliswa;
2. Ayiqhudelani namashaneli e-amino acid, inezindawo eziningi zokumunca kanye nesivinini sokumunca ngokushesha;
3. Ukusetshenziswa kancane kwamandla; 4. Amadiphozithi amaningi, izinga eliphezulu lokusetshenziswa kanye nokwenza ngcono kakhulu ukukhiqizwa kwezilwane;
5. I-antibacterial kanye ne-antioxidant;
6. Ukulawulwa kwamasosha omzimba.
Inani elikhulu lezifundo libonise ukuthi izici ezingenhla noma imiphumela ye-peptide chelates encane ibenza babe namathemba abanzi okufaka isicelo namandla okuthuthuka, ngakho inkampani yethu ekugcineni yanquma ukuthatha ama-peptide chelates amancane njengokugxila kocwaningo nokuthuthukiswa komkhiqizo we-organic trace wenkampani.
Ingxenye 3 Ukusebenza kahle kwama-peptide chelates amancane
1.Ubudlelwano phakathi kwama-peptides, ama-amino acid namaprotheni
Isisindo samangqamuzana amaprotheni singaphezu kuka-10000;
Isisindo samangqamuzana e-peptide singama-150 ~ 10000;
Ama-peptide amancane, abizwa nangokuthi ama-peptide amangqamuzana amancane, aqukethe ama-amino acid angama-2 ~ 4;
Isilinganiso sesisindo samangqamuzana sama-amino acid singaba ngu-150.
2. Amaqembu okuxhumanisa ama-amino acid nama-peptide acwecwe ngezinsimbi
(1) Ukuxhumanisa amaqembu kuma-amino acid
Amaqembu okuxhumanisa kuma-amino acid:
Amaqembu e-amino ne-carboxyl ku-a-carbon;
Amaqembu amaketanga aseceleni amanye ama-amino acid, njengeqembu le-sulfhydryl le-cysteine, iqembu le-phenolic le-tyrosine neqembu le-imidazole le-histidine.
(2) Ukuxhumanisa amaqembu kuma-peptide amancane
Ama-peptide amancane anamaqembu amaningi okuxhumanisa kunama-amino acid. Uma zichela ngama-ion ensimbi, kulula ukuchelate, futhi zingakha i-multidentate chelation, eyenza i-chelate izinze.
3. Ukusebenza komkhiqizo omncane we-peptide chelate
Isisekelo setiyetha se-peptide encane ekhuthaza ukumuncwa kwamaminerali okulandela umkhondo
Izici zokumuncwa zama-peptide amancane ziyisisekelo sethiyori sokuthuthukisa ukumuncwa kwezakhi zokulandelela. Ngokombono wendabuko we-protein metabolism, lokho izilwane ezikudingayo ukuze uthole amaprotheni yilokho ezikudingayo kuma-amino acid ahlukahlukene. Kodwa-ke, eminyakeni yamuva nje, ucwaningo luye lwabonisa ukuthi isilinganiso sokusetshenziswa kwama-amino acids ekudleni okuvela emithonjeni ehlukene sihlukile, futhi lapho izilwane zondliwa ngokudla okune-homozygous noma ukudla okune-protein ephansi ye-amino acid elinganiselayo, ukusebenza kahle kokukhiqiza akukwazi ukutholakala (Baker, 1977; Pinchasov et al., 1990) [2,3]. Ngakho-ke, ezinye izazi zibeka phambili umbono wokuthi izilwane zinamandla akhethekile okumunca amaprotheni ngokwawo angaphelele noma ama-peptide ahlobene. U-Agar(1953)[4] waqala waqaphela ukuthi umgudu wamathumbu ungamunca ngokuphelele futhi uhambise i-diglycidyl. Kusukela ngaleso sikhathi, abacwaningi baye babeka phambili impikiswano eqinisekisayo yokuthi ama-peptide amancane angamuncwa ngokuphelele, eqinisekisa ukuthi i-glycylglycine eqinile iyathuthwa futhi imuncwe; Inani elikhulu lama-peptide amancane lingamuncwa ngokuqondile ekujikelezeni kwesistimu ngendlela yama-peptide. Hara et al. (1984)[5] uphinde waveza ukuthi imikhiqizo yokugcina yokugaya amaprotheni emgudwini wokugaya ukudla iningi lama-peptide amancane kunama-amino acid amahhala (FAA). Ama-peptide amancane angadlula kumaseli e-mucosal emathunjini ngokuphelele futhi angene ku-systemic circulation (Le Guowei, 1996)[6].
Inqubekelaphambili Yocwaningo Lwe-Peptide Encane Ekhuthaza Ukumuncwa Kwamaminerali E-Trace, Qiao Wei, et al.
Ama-peptide chelates amancane ahanjiswa futhi amuncwa ngendlela yama-peptide amancane
Ngokusho kwendlela yokumuncwa kanye neyokuthutha kanye nezici zama-peptide amancane, landelela amaminerali e-chelate anama-peptide amancane njengoba ama-ligands ayinhloko angase ahanjiswe ewonke, okusiza kakhulu ekuthuthukiseni amandla e-biological of trace minerals. (Qiao Wei, et al)
Ukusebenza Kwe-Peptide Chelates Encane
1. Lapho ama-peptide amancane e-chelate nama-ion ensimbi, acebile ngamafomu futhi anzima ukugcwaliswa;
2. Ayiqhudelani namashaneli e-amino acid, inezindawo eziningi zokumunca kanye nesivinini sokumunca ngokushesha;
3. Ukusetshenziswa kancane kwamandla;
4. Amadiphozithi amaningi, izinga eliphezulu lokusetshenziswa kanye nokwenza ngcono kakhulu ukukhiqizwa kwezilwane;
5. I-antibacterial kanye ne-antioxidant; 6. Ukulawulwa kwamasosha omzimba.
4. Ukuqonda okwengeziwe kwama-peptides
Ibaphi kulaba basebenzisi ababili be-peptide abathola imali eyengeziwe?
- I-peptide ebophayo
- I-Phosphopeptide
- Ama-reagents ahlobene
- I-peptide ye-antimicrobial
- I-peptide yamasosha omzimba
- I-Neuropeptide
- I-Hormone peptide
- I-Antioxidant peptide
- Ama-peptide omsoco
- Ama-peptides okuphuza
(1) Ukuhlukaniswa kwama-peptides
(2) Imiphumela ye-physiological yama-peptides
- 1. Lungisa ibhalansi yamanzi ne-electrolyte emzimbeni;
- 2. Yenza amasosha omzimba alwa namagciwane kanye nezifo ukuze amasosha omzimba athuthukise ukusebenza kwawo;
- 3. Khuthaza ukuphulukiswa kwesilonda; Ukulungiswa okusheshayo kokulimala kwezicubu ze-epithelial.
- 4. Ukwenza ama-enzyme emzimbeni kusiza ekuguquleni ukudla kube amandla;
- 5. Ukulungisa amangqamuzana, uthuthukise umzimba wamangqamuzana, uvimbele ukuwohloka kwamangqamuzana, futhi ubambe iqhaza ekuvimbeleni umdlavuza;
- 6. Khuthaza ukuhlanganiswa nokulawulwa kwamaprotheni nama-enzyme;
- 7. Isithunywa samakhemikhali esibalulekile sokuxhumana phakathi kwamaseli nezitho;
- 8. Ukuvimbela izifo zenhliziyo kanye ne-cerebrovascular;
- 9. Lawula uhlelo lwe-endocrine kanye nezinzwa.
- 10. Thuthukisa uhlelo lokugaya ukudla futhi welaphe izifo ezingelapheki zamathumbu;
- 11. Thuthukisa isifo sikashukela, i-rheumatism, i-rheumatoid nezinye izifo.
- 12. Ukutheleleka ngegciwane, ukulwa nokuguga, ukuqedwa kwama-radicals mahhala emzimbeni.
- 13. Thuthukisa ukusebenza kwe-hematopoietic, ukwelapha i-anemia, ukuvimbela ukuhlangana kwe-platelet, okungathuthukisa amandla okuthwala umoya-mpilo wamangqamuzana abomvu egazi.
- 14. Yilwa ngokuqondile namagciwane e-DNA futhi uqondise amagciwane angama-viral.
5. Ukusebenza okubili okunomsoco we-peptide chelates encane
I-peptide chelate encane ingena esitokisini sisonke emzimbeni wesilwane, futhibese iphula ngokuzenzakalelayo isibopho se-chelationkuseli bese ibola ibe yi-peptide ne-ion yensimbi, esetshenziswa ngokulandelanaisilwane ukudlala imisebenzi emibili yokudla okunempilo, ikakhulukazi iumsebenzi we-peptide.
Umsebenzi we-peptide encane
- 1.Thuthukisa ukwakheka kwamaprotheni ezicutshini zemisipha yezilwane, wehlise i-apoptosis, futhi ukhuthaze ukukhula kwezilwane
- 2.Thuthukisa ukwakheka kwezimbali zamathumbu futhi ukhuthaze impilo yamathumbu
- 3.Nikeza i-carbon skeleton futhi ukhulise umsebenzi wama-enzymes wokugaya njenge-amylase yamathumbu kanye ne-protease
- 4.Iba nemiphumela yokucindezeleka elwa ne-oxidative
- 5.Ibe nezindawo zokuqeda ukuvuvukala
- 6.……
6. Izinzuzo zama-peptide chelates amancane ngaphezu kwama-amino acid chelates
| Amino acid chelated trace amaminerali | Amaminerali amancane e-peptide chelated trace | |
| Izindleko zezinto ezingavuthiwe | Izinto zokusetshenziswa ze-amino acid eyodwa ziyabiza | Izinto zokusetshenziswa ze-keratin zaseChina ziningi. Izinwele, izinselo nezimpondo ekufuyweni kwezilwane kanye namaprotheni amanzi angcolile kanye nezinsalela zesikhumba embonini yamakhemikhali yizinto ezisetshenziswayo ezisezingeni eliphezulu futhi ezishibhile zamaprotheni. |
| Umphumela wokumuncwa | Amaqembu e-amino kanye ne-carboxyl ahileleke kanyekanye ekwakhiweni kwama-amino acid nezakhi zensimbi, akha isakhiwo se-bicyclic endocannabinoid esifana nesama-dipeptides, ngaphandle kwamaqembu amahhala e-carboxyl akhona, angamuncwa kuphela ngohlelo lwe-oligopeptide. (Su Chunyang et al., 2002) | Lapho ama-peptide amancane ebamba iqhaza ku-chelation, isakhiwo se-chelation esiyindandatho esisodwa ngokuvamile sakhiwa iqembu le-amino elibulalayo kanye nomoya-mpilo wesibopho se-peptide eseduze, futhi i-chelate igcina iqembu lamahhala le-carboxyl, elingamuncwa ngohlelo lwe-dipeptide, olunomfutho ophakeme kakhulu wokumunca kunohlelo lwe-oligopeptide. |
| Ukuzinza | Ama-ion ensimbi anendandatho eyodwa noma ngaphezulu enamalungu amahlanu noma ayisithupha yamaqembu e-amino, amaqembu e-carboxyl, amaqembu e-imidazole, amaqembu e-phenol, namaqembu e-sulfhydryl. | Ngaphezu kwamaqembu amahlanu akhona wokuhlanganisa ama-amino acid, amaqembu e-carbonyl nama-imino kuma-peptide amancane nawo angabandakanyeka ekusebenzisaneni, ngaleyo ndlela enze ama-peptide chelates azinze kakhulu kunama-amino acid chelates. (Yang Pin et al., 2002) |
7. Izinzuzo zama-peptide chelates amancane ngaphezu kwe-glycolic acid ne-methionine chelates
| I-Glycine chelated trace minerals | I-Methionine chelated trace minerals | Amaminerali amancane e-peptide chelated trace | |
| Ifomu lokuxhumanisa | Amaqembu e-carboxyl nama-amino e-glycine angahlanganiswa nama-ion ensimbi. | Amaqembu e-carboxyl nama-amino e-methionine angaxhunyaniswa nama-ion ensimbi. | Uma ifakwe ama-ion ensimbi, inothile ngamafomu okuxhumanisa futhi ayisuthi kalula. |
| Umsebenzi wokudla okunomsoco | Izinhlobo nemisebenzi yama-amino acid iyodwa. | Izinhlobo nemisebenzi yama-amino acid iyodwa. | Iizinhlobonhlobo ezicebileama-amino acids ahlinzeka ngokudla okunomsoco ophelele, kuyilapho ama-peptide amancane angasebenza ngokufanele. |
| Umphumela wokumuncwa | I-Glycine chelates inazonoamaqembu amahhala e-carboxyl akhona futhi anomphumela wokumunca kancane. | Kukhona i-methionine chelatesnoamaqembu amahhala e-carboxyl akhona futhi anomphumela wokumunca kancane. | Ama-peptide chelate amancane akhekaqukathaukuba khona kwamaqembu e-carboxyl yamahhala futhi abe nomphumela wokumunca ngokushesha. |
Ingxenye 4 Igama Lokuhweba "I-Peptide-mineral Chelates Encane"
I-Chelates encane ye-Peptide-mineral, njengoba igama liphakamisa, kulula ukuchelate.
Kusho imigqa emincane ye-peptide, engagcwali kalula ngenxa yenani elikhulu lamaqembu wokuxhumanisa, Kulula ukwenza i-multidentate chelate enezici zensimbi, ngokuzinza okuhle.
Ingxenye 5 Isingeniso Semikhiqizo Encane Ye-Peptide-mineral Chelates Series
1. I-peptide encane ilandelela i-mineral chelated copper (igama lokuhweba: I-Copper Amino Acid Chelate Feed Grade)
2. I-peptide encane ilandelela i-mineral chelated iron (igama lokuhweba: I-Ferrous Amino Acid Chelate Feed Grade)
3. I-peptide encane ilandela i-mineral chelated zinc (igama lokuhweba: Zinc Amino Acid Chelate Feed Grade)
4. I-peptide encane ilandelela i-mineral chelated manganese (igama lokuhweba: Manganese Amino Acid Chelate Feed Grade)
I-Copper Amino Acid Chelate Yokuphakelayo Ibanga
Ibanga Lokuphakelayo kwe-Amino Acid Chelate
Zinc Amino Acid Chelate Okuphakelayo Ibanga
Manganese Amino Acid Chelate Okuphakelayo Ibanga
1. IBanga lokuphakelayo kweCopper Amino Acid Chelate
- Igama Lomkhiqizo: Ibanga Le-Copper Amino Acid Chelate Feed
- Ukubukeka: Ama-granules aluhlaza okwesibhakabhaka
- Imingcele ye-Physicochemical
a) Ithusi: ≥ 10.0%
b) Isamba sama-amino acid: ≥ 20.0%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) Umthofu: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Okuqukethwe komswakama: ≤ 5.0%
h) Ukulunga: Zonke izinhlayiya zidlula kuma-mesh angama-20, ezinosayizi wezinhlayiyana eziyinhloko ezingama-60-80 mesh
n=0,1,2,... ikhombisa ithusi elichelated lama-dipeptides, tripeptides, kanye ne-tetrapeptides
I-Diglycerin
Ukwakheka kwama-peptide chelates amancane
Izici ze-Copper Amino Acid Chelate Feed Grade
- Lo mkhiqizo uyi-all-organic trace mineral chelated by a special chelating process with pure plant enzymatic small molecule peptides as chelating substrates and trace elements.
- Lo mkhiqizo uzinzile kumakhemikhali futhi unganciphisa kakhulu umonakalo wawo kumavithamini namafutha, njll.
- Ukusetshenziswa kwalo mkhiqizo kusiza ekuthuthukiseni izinga lokuphakelayo. Umkhiqizo udonswa ngezindlela ezincane ze-peptide kanye ne-amino acid, wehlisa ukuncintisana kanye nokuphikisana nezinye izakhi zokulandelela, futhi unezinga elingcono kakhulu lokumuncwa kanye nokusetshenziswa kwe-bio.
- Ithusi liyingxenye eyinhloko yamangqamuzana egazi abomvu, izicubu ezixhumene, ithambo, elihilelekile emzimbeni wezinhlobonhlobo zama-enzyme, lithuthukisa ukuzivikela komzimba, umphumela wama-antibiotic, ungakhuphula ukuzuza kwesisindo sansuku zonke, uthuthukise inkokhelo yokuphakelayo.
Ukusetshenziswa kanye Nempumelelo Yebanga Le-Copper Amino Acid Chelate Feed
| Into yohlelo lokusebenza | Umthamo ophakanyisiwe (g/t inani eliphelele lezinto) | Okuqukethwe kokuphakelayo kwenani eligcwele (mg/kg) | Ukusebenza kahle |
| Hlanyela | 400-700 | 60-105 | 1. Ukwenza ngcono ukuzala kanye neminyaka yokusebenzisa kwezingulube; 2. Khulisa ubungqabavu bama-fetus kanye nezingulube; 3. Ukwenza ngcono ukuzivikela komzimba kanye nokumelana nezifo. |
| Ingulube yengulube | 300-600 | 45; 90 | 1. Inenzuzo ekuthuthukiseni imisebenzi ye-hematopoietic kanye ne-immune, ithuthukise ukumelana nokucindezeleka nokumelana nezifo; 2. Khulisa izinga lokukhula futhi uthuthukise kakhulu ukusebenza kahle kokuphakelayo. |
| Izingulube ezikhuluphalisayo | 125 | Januwari 18.5 | |
| Inyoni | 125 | Januwari 18.5 | 1. Ukwenza ngcono ukumelana nokucindezeleka futhi kunciphise ukufa; 2. Thuthukisa isinxephezelo sokuphakelayo futhi andise izinga lokukhula. |
| Izilwane zasemanzini | Izinhlanzi 40-70 | 6 - 10.5 | 1. Ukuthuthukisa ukukhula, ukuthuthukisa isinxephezelo sokudla; 2. Anti-stress, nciphisa ukugula nokufa. |
| I-Shrimp 150 ~ 200 | 22.5-30 | ||
| Isilwane esisabisayo g/usuku lwekhanda | Januwari 0.75 | 1. Vimbela ukuguqulwa kwamalunga e-tibial, ukuphazamiseka kokunyakaza kwe-"concave back", i-wobbler, ukulimala kwemisipha yenhliziyo; 2. Vimbela izinwele noma ijazi i-keratinization, ube izinwele ezinzima, ulahlekelwe ukugoba okuvamile, uvimbele ukuvela "kwezindawo ezimpunga" kumbuthano wamehlo; 3. Vimbela ukwehla kwesisindo, isifo sohudo, ukukhiqizwa kobisi Nciphisa. |
2. Ibanga Lokuphakelayo kwe-Amino Acid Esakhiweni
- Igama Lomkhiqizo: Ibanga Lokuphakelayo kwe-Ferrous Amino Acid Chelate
- Ukubukeka: Ama-granules aluhlaza okwesibhakabhaka
- Imingcele ye-Physicochemical
a) Insimbi: ≥ 10.0%
b) Isamba sama-amino acid: ≥ 19.0%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) Umthofu: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Okuqukethwe komswakama: ≤ 5.0%
h) Ukulunga: Zonke izinhlayiya zidlula kuma-mesh angama-20, ezinosayizi wezinhlayiyana eziyinhloko ezingama-60-80 mesh
n=0,1,2,...ikhombisa i-zinc chelated yama-dipeptides, tripeptides, kanye ne-tetrapeptides
Izici ze-Ferrous Amino Acid Chelate Feed Grade
- Lo mkhiqizo uyi-organic trace mineral chelated by a special chelating process with pure plant enzymatic small molecule peptides as chelating substrates and trace elements;
- Lo mkhiqizo uzinzile kumakhemikhali futhi unganciphisa kakhulu umonakalo wawo kumavithamini namafutha, njll. Ukusetshenziswa kwalo mkhiqizo kulungele ukuthuthukisa izinga lokudla;
- Umkhiqizo udonswa ngezindlela ezincane ze-peptide ne-amino acid, unciphisa ukuncintisana kanye nokuphikisana nezinye izakhi zokulandelela, futhi unezinga elingcono kakhulu lokumuncwa kanye nokusetshenziswa kwe-bio;
- Lo mkhiqizo ungadlula kumgoqo we-placenta kanye nendlala yebele, wenze umbungu ube nempilo enhle, ukhulise isisindo sokuzalwa kanye nesisindo sokulunyulwa, futhi unciphise izinga lokufa; I-ayoni iyingxenye ebalulekile ye-hemoglobin ne-myoglobin, engavimbela ngempumelelo i-anemia yokuntuleka kwensimbi kanye nezinkinga zayo.
Ukusetshenziswa kanye Nempumelelo Yebanga Le-Ferrous Amino Acid Chelate Feed
| Into yohlelo lokusebenza | Umthamo ophakanyisiwe (g/t inani eliphelele lempahla) | Okuqukethwe kokuphakelayo kwenani eligcwele (mg/kg) | Ukusebenza kahle |
| Hlanyela | 300-800 | 45-120 | 1. Ukwenza ngcono ukuzala kanye nempilo yokusebenzisa kwezingulube; 2. ukuthuthukisa leso sisindo sokuzalwa, isisindo sokulunyulwa kanye nokufana kwengulube ukuze ikhiqize kangcono esikhathini esizayo; 3. Thuthukisa ukugcinwa kwe-ayoni ezingulubeni ezincelayo kanye nokugcwala kwe-ayoni obisini ukuze kuvinjelwe i-anemia yokuntuleka kwe-iron ezingulubeni ezincelayo. |
| Izingulube nezingulube ezikhuluphalisayo | Izingulube 300 ~ 600 | 45; 90 | 1. Ukuthuthukisa ukuvikeleka kwamantshontsho ezingulube, ukuthuthukisa ukumelana nezifo kanye nokwenza ngcono izinga lokusinda; 2. Khulisa izinga lokukhula, uthuthukise ukuguqulwa kwesiphakeli, ukhulise isisindo sokulunyulwa kanye nokufana, futhi unciphise izehlakalo zezingulube ezigulayo; 3. Thuthukisa izinga le-myoglobin ne-myoglobin, uvimbele futhi welaphe i-anemia yokuntuleka kwensimbi, wenze isikhumba sengulube sibe bomvu futhi ngokusobala sithuthukise umbala wenyama. |
| Ukukhuluphalisa izingulube 200 ~ 400 | 30 - 60 | ||
| Inyoni | 300-400 | 45; 60 | 1. Thuthukisa ukuguqulwa kokuphakelayo, ukhuphule izinga lokukhula, uthuthukise ikhono lokulwa nokucindezeleka futhi unciphise ukufa; 2. Thuthukisa izinga lokubeka amaqanda, unciphise izinga leqanda eliphukile futhi ujulise umbala we-yolk; 3. Thuthukisa izinga lokuzala kanye nezinga lokuchanyuselwa kwamaqanda azalela kanye nezinga lokusinda kwezinkukhu ezisencane. |
| Izilwane zasemanzini | 200-300 | 30-45 | 1. Khuthaza ukukhula, uthuthukise ukuguqulwa kwesiphakeli; 2. Ukuthuthukisa ukuqeda ingcindezi, ukunciphisa ukugula nokufa. |
3. Zinc Amino Acid Chelate Okuphakelayo Grade
- Igama Lomkhiqizo: Zinc Amino Acid Chelate Okuphakelayo Ibanga
- Ukubukeka: ama-granules ansundu ngokuphuzi
- Imingcele ye-Physicochemical
a) Zinc: ≥ 10.0%
b) Isamba sama-amino acid: ≥ 20.5%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) Umthofu: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Okuqukethwe komswakama: ≤ 5.0%
h) Ukulunga: Zonke izinhlayiya zidlula kuma-mesh angama-20, ezinosayizi wezinhlayiyana eziyinhloko ezingama-60-80 mesh
n=0,1,2,...ikhombisa i-zinc chelated yama-dipeptides, tripeptides, kanye ne-tetrapeptides
Izici ze-Zinc Amino Acid Chelate Feed Grade
Lo mkhiqizo uyi-all-organic trace mineral chelated by a special chelating process with pure plant enzymatic small molecule peptides as chelating substrates and trace elements;
Lo mkhiqizo uzinzile kumakhemikhali futhi unganciphisa kakhulu umonakalo wawo kumavithamini namafutha, njll.
Ukusetshenziswa kwalo mkhiqizo kusiza ekuthuthukiseni izinga lokudla; Umkhiqizo udonswa ngezindlela ezincane ze-peptide ne-amino acid, unciphisa ukuncintisana kanye nokuphikisana nezinye izakhi zokulandelela, futhi unezinga elingcono kakhulu lokumuncwa kanye nokusetshenziswa kwe-bio;
Lo mkhiqizo ungathuthukisa ukungatheleleki, ukhuthaze ukukhula, ukwandise ukuguqulwa kokuphakelayo futhi uthuthukise isicwebezelisi soboya;
I-Zinc iyisakhi esibalulekile sama-enzyme angaphezu kwama-200, izicubu ze-epithelial, i-ribose ne-gustatin. Ikhuthaza ukwanda okusheshayo kwamangqamuzana okunambitha ku-mucosa yolimi futhi ilawula ukudla; ivimbela amagciwane ayingozi emathunjini; futhi inomsebenzi wama-antibiotics, ongathuthukisa umsebenzi wokuthungatha wesistimu yokugaya ukudla kanye nomsebenzi wama-enzyme ezicubu namaseli.
Ukusetshenziswa kanye Nempumelelo Yebanga Le-Zinc Amino Acid Chelate Feed
| Into yohlelo lokusebenza | Umthamo ophakanyisiwe (g/t inani eliphelele lempahla) | Okuqukethwe kokuphakelayo kwenani eligcwele (mg/kg) | Ukusebenza kahle |
| Izingulube ezikhulelwe nezincelisayo | 300-500 | 45; 75 | 1. Ukwenza ngcono ukuzala kanye nempilo yokusebenzisa kwezingulube; 2. Thuthukisa ubungqabavu be-fetus namaphuphu, uthuthukise ukumelana nezifo, futhi uwenze abe nokusebenza kangcono kokukhiqiza esikhathini sakamuva; 3. Thuthukisa isimo somzimba wengulube ekhulelwe kanye nesisindo sokuzalwa kwamaphuphu. |
| Ingulube encelisayo, ingulube kanye nezingulube ezikhulayo ezikhuluphalisayo | 250-400 | 37.5-60 | 1. Ukwenza ngcono ukuvikeleka kwezingulube, ukunciphisa isifo sohudo nokufa; 2. Ukwenza ngcono ukunambitheka, ukwandisa ukudla okudliwayo, ukwandisa izinga lokukhula kanye nokwenza ngcono ukuguqulwa kokuphakelayo; 3. Yenza ijazi lengulube likhanye futhi uthuthukise ikhwalithi yesidumbu kanye nekhwalithi yenyama. |
| Inyoni | 300-400 | 45; 60 | 1. Thuthukisa ukucwebezela kwezimpaphe; 2. ukuthuthukisa izinga lokuzalela, izinga lokuvundiswa kanye nezinga lokuchanyuselwa lokuzalanisa amaqanda, futhi kuqinise ikhono lokufaka imibala lesikhupha seqanda; 3. Ukuthuthukisa ikhono lokulwa nokucindezeleka futhi kunciphise ukufa; 4. Thuthukisa ukuguqulwa kokuphakelayo futhi ukhuphule izinga lokukhula. |
| Izilwane zasemanzini | Januwari 300 | 45 | 1. Khuthaza ukukhula, uthuthukise ukuguqulwa kwesiphakeli; 2. Ukuthuthukisa ukuqeda ingcindezi, ukunciphisa ukugula nokufa. |
| Isilwane esisabisayo g/usuku lwekhanda | 2.4 | 1. Ukwenza ngcono ukukhiqizwa kobisi, kuvimbele i-mastitis nokubola kwe-foof, futhi kunciphise okuqukethwe kwe-somatic cell obisini; 2. Khuthaza ukukhula, uthuthukise ukuguqulwa kwesiphakeli futhi uthuthukise ikhwalithi yenyama. |
4. Manganese Amino Acid Chelate Feed Grade
- Igama Lomkhiqizo: Manganese Amino Acid Chelate Okuphakelayo Ibanga
- Ukubukeka: ama-granules ansundu ngokuphuzi
- Imingcele ye-Physicochemical
a) Mn: ≥ 10.0%
b) Isamba sama-amino acid: ≥ 19.5%
c) Izinga le-Chelation: ≥ 95%
d) I-Arsenic: ≤ 2 mg/kg
e) Umthofu: ≤ 5 mg/kg
f) I-Cadmium: ≤ 5 mg/kg
g) Okuqukethwe komswakama: ≤ 5.0%
h) Ukulunga: Zonke izinhlayiya zidlula kuma-mesh angama-20, ezinosayizi wezinhlayiyana eziyinhloko ezingama-60-80 mesh
n=0, 1,2,...ikhombisa i-chelated manganese kuma-dipeptides, tripeptides, kanye ne-tetrapeptides
Izici Zebanga Le-Manganese Amino Acid Chelate Okuphakelayo
Lo mkhiqizo uyi-all-organic trace mineral chelated by a special chelating process with pure plant enzymatic small molecule peptides as chelating substrates and trace elements;
Lo mkhiqizo uzinzile kumakhemikhali futhi unganciphisa kakhulu umonakalo wawo kumavithamini namafutha, njll. Ukusetshenziswa kwalo mkhiqizo kulungele ukuthuthukisa izinga lokudla;
Umkhiqizo udonswa ngezindlela ezincane ze-peptide ne-amino acid, unciphisa ukuncintisana kanye nokuphikisana nezinye izakhi zokulandelela, futhi unezinga elingcono kakhulu lokumuncwa kanye nokusetshenziswa kwe-bio;
Umkhiqizo ungathuthukisa izinga lokukhula, uthuthukise ukuguqulwa kokuphakelayo kanye nesimo sezempilo kakhulu; futhi kuthuthukiswe izinga lokuzalela, izinga lokuchanyuselwa kanye nezinga elinempilo lokuzalanisa izinkukhu ngokusobala;
I-Manganese iyadingeka ekukhuleni kwamathambo kanye nokugcinwa kwezicubu ezixhumeneyo. Ihlobene eduze nama-enzyme amaningi; futhi ubamba iqhaza kuma-carbohydrate, amafutha kanye namaprotheni umzimba, ukukhiqiza kanye nokusabela komzimba.
Ukusetshenziswa kanye Nempumelelo Yebanga Le-Manganese Amino Acid Chelate Feed
| Into yohlelo lokusebenza | Umthamo ophakanyisiwe (g/t inani eliphelele lezinto) | Okuqukethwe kokuphakelayo kwenani eligcwele (mg/kg) | Ukusebenza kahle |
| Ingulube yokuzalanisa | 200-300 | 30-45 | 1. Khuthaza ukukhula okuvamile kwezitho zocansi futhi uthuthukise ukuhamba kwesidoda; 2. Thuthukisa amandla okuzala ezingulube ezizalanisa futhi unciphise izithiyo zokuzala. |
| Izingulube nezingulube ezikhuluphalisayo | 100 - 250 | 15 - 37.5 | 1. Kuyazuzisa ukuthuthukisa imisebenzi yokuzivikela komzimba, nokuthuthukisa ikhono lokulwa nokucindezeleka kanye nokumelana nezifo; 2. Khuthaza ukukhula futhi uthuthukise ukuguqulwa kwesiphakeli kakhulu; 3. Thuthukisa umbala nekhwalithi yenyama, futhi uthuthukise amaphesenti enyama engenamafutha. |
| Inyoni | 250 - 350 | 37.5-52.5 | 1. Ukuthuthukisa ikhono lokulwa nokucindezeleka futhi kunciphise ukufa; 2. Ukwenza ngcono izinga lokuzalela, izinga lokuvundiswa kanye nezinga lokuchanyuselwa kwamaqanda azalela, thuthukisa ikhwalithi yegobolondo leqanda futhi wehlise izinga lokuphuka kwamagobolondo; 3. Khuthaza ukukhula kwamathambo futhi unciphise izifo zemilenze. |
| Izilwane zasemanzini | 100-200 | 15 - 30 | 1. Khuthaza ukukhula futhi uthuthukise ikhono layo lokulwa nokucindezeleka kanye nokumelana nezifo; 2. Thuthukisa ukuhamba kwesidoda kanye nezinga lokuchanyuselwa kwamaqanda avundisiwe. |
| Isilwane esisabisayo g/usuku lwekhanda | Izinkomo 1.25 | 1. Vimbela ukuphazamiseka kwe-fatty acid synthesis kanye nokulimala kwezicubu zethambo; 2. Ukuthuthukisa amandla okuzala, ukuvimbela ukuhushulwa kwezisu kanye nokukhubazeka kwangemva kokubeletha kwezilwane ezinsikazi, ukunciphisa ukufa kwamathole namawundlu, futhi andise isisindo esisanda kuzalwa sezilwane ezincane. | |
| Imbuzi 0.25 |
Ingxenye 6 ye-FAB ye-Small Peptide-mineral Chelates
| I-S/N | F: Izibaluli zokusebenza | A: Umehluko wokuncintisana | B: Izinzuzo ezilethwa umehluko wokuncintisana kubasebenzisi |
| 1 | Ukulawula ukukhetha kwezinto zokusetshenziswa | Khetha isitshalo esihlanzekile se-enzymatic hydrolysis yama-peptide amancane | Ukuphepha okuphezulu kwezinto eziphilayo, ukugwema ubuzimu |
| 2 | Ubuchwepheshe bokugaya ukudla okuqondisayo kwe-enzyme yebhayoloji yamaprotheni amabili | Ingxenye ephezulu yama-peptide amangqamuzana amancane | Okuningi "okuhlosiwe", okungelula ukugcwaliswa, ngokusebenza okuphezulu kwezinto eziphilayo nokuzinza okungcono |
| 3 | I-Advanced pressure spray & drying technology | Umkhiqizo oyimbudumbudu, onosayizi wezinhlayiyana ezifanayo, uketshezi olungcono, akulula ukumunca umswakama | Qinisekisa ukuthi kulula ukuyisebenzisa, ukuxuba okufanayo okuphakelayo okuphelele |
| Okuqukethwe kwamanzi aphansi (≤ 5%), okunciphisa kakhulu ithonya elibangelwa amavithamini namalungiselelo e-enzyme | Thuthukisa ukuzinza kwemikhiqizo yokuphakelayo | ||
| 4 | Ubuchwepheshe bokulawula ukukhiqiza obusezingeni eliphezulu | Inqubo evalwe ngokuphelele, izinga eliphezulu lokulawula okuzenzakalelayo | Ikhwalithi ephephile futhi ezinzile |
| 5 | Ubuchwepheshe bokulawula izinga eliphezulu | Sungula futhi uthuthukise izindlela zokuhlaziya zesayensi nezithuthukisiwe kanye nezindlela zokulawula zokuthola izinto ezithinta ikhwalithi yomkhiqizo, njengeprotheyini encibilikayo ene-asidi, ukusatshalaliswa kwesisindo samangqamuzana, ama-amino acid kanye nezinga le-chelating | Qinisekisa ikhwalithi, uqinisekise ukusebenza kahle futhi uthuthukise ukusebenza kahle |
Ingxenye 7 Ukuqhathaniswa Kwezimbangi
I-Standard VS Standard
Ukuqhathaniswa kokusatshalaliswa kwe-peptide kanye nezinga le-chelation lemikhiqizo
| Imikhiqizo ye-Sustar | Ingxenye yama-peptides amancane (180-500) | Imikhiqizo ye-Zinpro | Ingxenye yama-peptides amancane (180-500) |
| AA-Cu | ≥74% | I-AVAILA-Cu | 78% |
| AA-Fe | ≥48% | I-AVAILA-Fe | 59% |
| AA-Mn | ≥33% | AVAILA-Mn | 53% |
| AA-Zn | ≥37% | I-AVAILA-Zn | 56% |
| Imikhiqizo ye-Sustar | Izinga le-Chelation | Imikhiqizo ye-Zinpro | Izinga le-Chelation |
| AA-Cu | 94.8% | I-AVAILA-Cu | 94.8% |
| AA-Fe | 95.3% | I-AVAILA-Fe | 93.5% |
| AA-Mn | 94.6% | AVAILA-Mn | 94.6% |
| AA-Zn | 97.7% | I-AVAILA-Zn | 90.6% |
Isilinganiso sama-peptide amancane e-Sustar singaphansi kancane kune-Zinpro, futhi izinga lokushelela lemikhiqizo ye-Sustar lingaphezulu kancane kwelemikhiqizo ye-Zinpro.
Ukuqhathaniswa kokuqukethwe kwama-amino acid ayi-17 emikhiqizweni ehlukene
| Igama lika ama-amino acid | I-Sustar's Copper I-Amino Acid Chelate Okuphakelayo Ibanga | I-Zinpro AVAILA ithusi | I-Sustar's Ferrous Amino Acid C helate Okuphakelayo Ibanga | I-AVAILA ye-Zinpro insimbi | I-Sustar's Manganese I-Amino Acid Chelate Okuphakelayo Ibanga | I-AVAILA ye-Zinpro manganese | I-Zinc ye-Sustar I-Amino Acid Ibanga le-Chelate Feed | I-AVAILA ye-Zinpro zinc |
| i-aspartic acid (%) | 1.88 | 0.72 | 1.50 | 0.56 | 1.78 | 1.47 | 1.80 | 2.09 |
| i-glutamic acid (%) | 4.08 | 6.03 | 4.23 | 5.52 | 4.22 | 5.01 | 4.35 | 3.19 |
| I-Serine (%) | 0.86 | 0.41 | 1.08 | 0.19 | 1.05 | 0.91 | 1.03 | 2.81 |
| I-Histidine (%) | 0.56 | 0.00 | 0.68 | 0.13 | 0.64 | 0.42 | 0.61 | 0.00 |
| I-Glycine (%) | 1.96 | 4.07 | 1.34 | 2.49 | 1.21 | 0.55 | 1.32 | 2.69 |
| I-Threonine (%) | 0.81 | 0.00 | 1.16 | 0.00 | 0.88 | 0.59 | 1.24 | 1.11 |
| I-Arginine (%) | 1.05 | 0.78 | 1.05 | 0.29 | 1.43 | 0.54 | 1.20 | 1.89 |
| I-Alanine (%) | 2.85 | 1.52 | 2.33 | 0.93 | 2.40 | 1.74 | 2.42 | 1.68 |
| I-Tyrosinase (%) | 0.45 | 0.29 | 0.47 | 0.28 | 0.58 | 0.65 | 0.60 | 0.66 |
| I-cystinol (%) | 0.00 | 0.00 | 0.09 | 0.00 | 0.11 | 0.00 | 0.09 | 0.00 |
| I-Valine (%) | 1.45 | 1.14 | 1.31 | 0.42 | 1.20 | 1.03 | 1.32 | 2.62 |
| I-Methionine (%) | 0.35 | 0.27 | 0.72 | 0.65 | 0.67 | 0.43 | Januwari 0.75 | 0.44 |
| I-Phenylalanine (%) | 0.79 | 0.41 | 0.82 | 0.56 | 0.70 | 1.22 | 0.86 | 1.37 |
| Isoleucine (%) | 0.87 | 0.55 | 0.83 | 0.33 | 0.86 | 0.83 | 0.87 | 1.32 |
| I-Leucine (%) | 2.16 | 0.90 | 2.00 | 1.43 | 1.84 | 3.29 | 2.19 | 2.20 |
| I-Lysine (%) | 0.67 | 2.67 | 0.62 | 1.65 | 0.81 | 0.29 | 0.79 | 0.62 |
| I-Proline (%) | 2.43 | 1.65 | 1.98 | 0.73 | 1.88 | 1.81 | 2.43 | 2.78 |
| Isamba sama-amino acid (%) | 23.2 | 21.4 | 22.2 | 16.1 | 22.3 | 20.8 | 23.9 | 27.5 |
Sekukonke, ingxenye yama-amino acid emikhiqizweni ye-Sustar iphezulu kunaleyo emikhiqizweni ye-Zinpro.
Ingxenye 8 Imiphumela yokusetshenziswa
Imiphumela yemithombo ehlukene yokulandela umkhondo wamaminerali ekusebenzeni kokukhiqiza kanye nekhwalithi yamaqanda ezinkukhu ezizalelayo ngasekupheleni kwesikhathi sokubekela
Inqubo Yokukhiqiza
- Ubuchwepheshe be-chelation obuhlosiwe
- Ubuchwepheshe be-shear emulsification
- I-pressure spray & drying technology
- Ubuchwepheshe bokuqandisa nokususa umswakama
- Ubuchwepheshe obusezingeni eliphezulu bokulawula imvelo
I-Appendix A: Izindlela Zokunqunywa kokusatshalaliswa kwe-molecular mass yama-peptide
Ukwamukelwa kwezinga: GB/T 22492-2008
1 Isimiso Sokuhlola:
Kwanqunywa ukusebenza okuphezulu kwe-gel filtration chromatography. Okusho ukuthi, kusetshenziswa i-porous filler njengesigaba esimile, ngokusekelwe emehlukweni kusayizi wamangqamuzana ohlobene wezingxenye zesampula zokuhlukaniswa, ezitholwe kubhondi ye-peptide yobude beza beza be-ultraviolet bokumuncwa obungu-220nm, kusetshenziswa isofthiwe yokucubungula idatha ezinikele ekunqumeni ukusatshalaliswa kwesisindo samangqamuzana ngejeli yokuhlunga kwe-chromatration, isofthiwe yokuhlunga idatha, i-chromatography yedatha, i-chromatography kubalwe ukuze kutholwe usayizi we-molecular mass ye-soya peptide kanye nobubanzi bokusabalalisa.
2. Ama-reagents
Amanzi okuhlola kufanele ahlangabezane nokucaciswa kwamanzi esibili ku-GB/T6682, ukusetshenziswa kwama-reagents, ngaphandle kwezinhlinzeko ezikhethekile, ahlanzekile ngokohlaziyo.
2.1 Ama-reagents afaka i-acetonitrile (i-chromatographically pure), i-trifluoroacetic acid (i-chromatographically pure),
2.2 Izinto ezijwayelekile ezisetshenziswa kwijika lokulinganiswa lokusatshalaliswa kwesisindo samangqamuzana: i-insulin, i-mycopeptides, i-glycine-glycine-tyrosine-arginine, i-glycine-glycine-glycine
3 Insimbi nezinto zokusebenza
3.1 I-High Performance Liquid Chromatograph (HPLC): indawo yokusebenza yechromatographic noma isihlanganisi esinomtshina we-UV kanye nesofthiwe yokucubungula idatha ye-GPC.
3.2 Iyunithi yokuhlunga kwe-vacuum yesigaba seselula kanye neyunithi yokukhipha umoya.
3.3 Ibhalansi ye-elekthronikhi: inani leziqu 0.000 1g.
4 Izinyathelo zokusebenza
4.1 Izimo ze-Chromatographic nokuhlolwa kokujwayela isistimu (izimo zereferensi)
4.1.1 Ikholomu ye-Chromatographic: TSKgelG2000swxl300 mm×7.8 mm (ububanzi bangaphakathi) noma amanye amakholomu ejeli ohlobo olufanayo ngokusebenza okufanayo okulungele ukunqunywa kwamaprotheni nama-peptide.
4.1.2 Isigaba seselula: I-Acetonitrile + amanzi + trifluoroacetic acid = 20 + 80 + 0.1.
4.1.3 Ubude begagasi bokutholwa: 220 nm.
4.1.4 Izinga lokugeleza: 0.5 mL/min.
4.1.5 Isikhathi sokutholwa: 30 min.
4.1.6 Isampula yevolumu yomjovo: 20μL.
4.1.7 Izinga lokushisa lekholomu: izinga lokushisa legumbi.
4.1.8 Ukuze kwenziwe isistimu ye-chromatographic ihlangabezane nezimfuneko zokutholwa, kwacaciswa ukuthi ngaphansi kwezimo zechromatographic ezingenhla, ukusebenza kahle kwekholomu ye-gel chromatographic, okungukuthi, inombolo yethiyori yamapuleti (N), yayingekho ngaphansi kuka-10000 abalwe ngesisekelo seziqongo ze-tripeptide standardly (Glycine-GlycineG).
4.2 Ukukhiqizwa kwamajika ajwayelekile e-molecular mass
Izisombululo ezingenhla ezihlukene zamangqamuzana e-peptide enesisindo esingu-1 mg/mL zalungiswa ngokufaniswa kwesigaba seselula, zaxutshwa ngengxenye ethile, zase zihlungwa ngolwelwesi lwesigaba sezinto eziphilayo ezinosayizi wembotshana ongu-0.2 μm~0.5 μm futhi zafakwa kusampula, kwase kutholwa ama-chromatogram ezindinganiso. Amajika okulinganisa ama-molecular mass kanye nezibalo zawo atholwe ngokuhlela i-logarithm yesisindo se-molecular mass ngokumelene nesikhathi sokugcinwa noma ngokuhlehla komugqa.
4.3 Ukwelashwa okuyisampula
Kala ngokunembile u-10mg wesampula ku-flask ye-volumetric engu-10mL, engeza isigaba esincane seselula, ukunyakaziswa kwe-ultrasonic imizuzu engu-10, ukuze isampula lihlakazwe ngokugcwele futhi lixutshwe, lihlanjululwe ngesigaba seselula esikalini, bese lihlungwa ngolwelwesi lwesigaba sezinto eziphilayo ezinosayizi we-pore ongu-0.2μm~0.5μm, futhi i-analychmatographic ibe yizimo ze-filter A.4.1.
5. Ukubalwa kokusabalalisa kwesisindo samangqamuzana
Ngemva kokuhlaziya isisombululo sesampula esilungiswe ngo-4.3 ngaphansi kwezimo ze-chromatographic ze-4.1, isisindo se-molecular mass yesampula kanye nobubanzi baso bokusabalalisa kungatholwa ngokufaka esikhundleni sedatha ye-chromatographic yesampula kukhevu yokulinganisa engu-4.2 ngesofthiwe yokucubungula idatha ye-GPC. Ukusatshalaliswa kwamangqamuzana ahlobene ama-peptide ahlukene angabalwa ngendlela yokujwayela yendawo ephakeme, ngokuya ngefomula: X=A/A ingqikithi×100
Efomini: X - Ingxenye enkulu ye-peptide ye-molecular mass peptide enanini le-peptide kusampula, %;
A - Indawo ephakeme kakhulu ye-peptide ye-molecular mass;
Ingqikithi A - isamba sezindawo eziphakeme kakhulu ze-peptide ye-molecular mass peptide, ibalwe endaweni eyodwa yedesimali.
6 Ukuphindaphinda
Umehluko ophelele phakathi kokunqunywa okubili okuzimele okutholwe ngaphansi kwezimo zokuphindaphinda ngeke kudlule u-15% wencazelo ye-arithmetic yokunquma kokubili.
Isithasiselo B: Izindlela Zokunqunywa Kwe-Amino Acid Yamahhala
Ukwamukelwa kwezinga: Q/320205 KAVN05-2016
1.2 Ama-reagents nezinto zokwakha
I-glacial acetic acid: ihlanzekile ngokuhlaziya
I-Perchloric acid: 0.0500 mol/L
Inkomba: 0.1% inkomba ye-crystal violet (glacial acetic acid)
2. Ukunqunywa kwama-amino acid amahhala
Amasampula omisiwe ku-80 ° C ihora elingu-1.
Beka isampula esitsheni esomile ukuze liphole ngokwemvelo ekamelweni lokushisa noma liphole liye ezingeni lokushisa elisebenzisekayo.
Kala cishe u-0.1 g wesampula (okunembe kuye ku-0.001 g) ube yi-250 mL yeflask ewukhonkolo eyomile.
Ngokushesha qhubekela esinyathelweni esilandelayo ukuze ugweme isampula ekumunceni umswakama we-ambient
Engeza u-25 mL we-glacial acetic acid futhi uhlanganise kahle isikhathi esingengaphezu kwemizuzu emi-5.
Engeza amaconsi angu-2 e-crystal violet indicator
Titrate ngo-0.0500 mol / L (±0.001) isixazululo esijwayelekile se-titration se-perchloric acid kuze kube yilapho isixazululo sishintsha sisuka kokunsomi siye ekugcineni.
Rekhoda umthamo wesixazululo esijwayelekile esisetshenzisiwe.
Yenza ukuhlolwa okungenalutho ngesikhathi esifanayo.
3. Ukubalwa kanye nemiphumela
Okuqukethwe kwe-amino acid yamahhala u-X ku-reagent kuvezwa njengengxenye enkulu (%) futhi ibalwa ngokuvumelana nefomula: X = C × (V1-V0) × 0.1445/M × 100%, ngefomula ethi:
C - Ukugxila kwesisombululo esijwayelekile se-perchloric acid kuma-moles ilitha ngalinye (i-mol/L)
I-V1 - Ivolumu esetshenziselwa ukulinganisa amasampula anesisombululo esijwayelekile se-perchloric acid, ngamamililitha (mL).
Ivolumu - Ivolumu esetshenziselwa ukusho lutho okungenalutho nesisombululo esijwayelekile se-perchloric acid, ngamamililitha (mL);
M - Isisindo sesampula, ngamagremu (g).
0.1445: Isilinganiso sesisindo sama-amino acid esilingana no-1.00 mL wesisombululo esijwayelekile se-perchloric acid [c (HClO4) = 1.000 mol / L].
I-Appendix C: Izindlela Zokunqunywa Kwezinga le-Chelation lika-Sustar
Ukwamukelwa kwamazinga: Q/70920556 71-2024
1. Isimiso sokunquma (Fe njengesibonelo)
Izakhiwo zensimbi ye-amino acid zinokuncibilika okuphansi kakhulu ku-ethanol enganamanzi futhi ama-ion ensimbi amahhala ancibilika ku-ethanol engenamanzi, umehluko wokuncibilika phakathi kwalokhu okubili ku-ethanol enganamanzi wasetshenziswa ukuze kunqunywe izinga le-chelation lama-amino acid iron complexes.
2. Ama-reagents nezisombululo
I-ethanol engenalutho; okunye kuyafana nesigatshana 4.5.2 ku-GB/T 27983-2011.
3. Izinyathelo zokuhlaziya
Yenza izivivinyo ezimbili ngokufana. Kala u-0.1g wesampula omisiwe ku-103±2℃ ihora elingu-1, okunembile kuya ku-0.0001g, engeza u-100mL we-ethanol engamanzi ukuze incibilike, isihlungi, izinsalela zokuhlunga zigezwe ngo-100mL we-ethanol engasebenzi okungenani izikhathi ezintathu, bese udlulisela insalela ye-150mL ye-cosmetology. isixazululo se-sulfuric acid ngokwesigatshana 4.5.3 ku-GB/T27983-2011, bese wenza izinyathelo ezilandelayo ngokwesigatshana 4.5.3 “Ukushisa ukuze kuncibilike bese uvumela ukupholisa” ku-GB/T27983-2011. Yenza ukuhlolwa okungenalutho ngesikhathi esifanayo.
4. Ukunqunywa kwengqikithi yensimbi
4.1 Umgomo wokunquma uyafana nesigatshana 4.4.1 ku-GB/T 21996-2008.
4.2. Ama-reagents nezixazululo
4.2.1 I-asidi exutshiwe: Engeza u-150mL we-sulfuric acid no-150mL we-phosphoric acid ku-700mL wamanzi futhi uhlanganise kahle.
4.2.2 Isixazululo senkomba ye-sodium diphenylamine sulfonate: 5g/L, elungiselelwe ngokuya nge-GB/T603.
4.2.3 Isixazululo se-titration esijwayelekile se-Cerium sulfate: ukuhlushwa c [Ce (SO4) 2] = 0.1 mol/L, okulungiselelwe ngokusho kwe-GB/T601.
4.3 Izinyathelo zokuhlaziya
Yenza izivivinyo ezimbili ngokufana. Isisindo esingu-0.1g sesampula, sinembile ku-020001g, faka ku-250mL ye-conical flask, engeza u-10mL we-asidi exutshwe, ngemva kokuhlakazwa, engeza u-30ml wamanzi namaconsi angu-4 esisombululo senkomba ye-sodium dianiline sulfonate, bese wenza lezi zinyathelo ezilandelayo ngokusho kwesigatshana 4.2108 ku-6 GB/T6. Yenza ukuhlolwa okungenalutho ngesikhathi esifanayo.
4.4 Ukumelelwa kwemiphumela
Ingqikithi yensimbi engu-X1 yezinhlanganisela zensimbi ye-amino acid ngokwengxenye enkulu yensimbi, inani elivezwe ngo-%, libalwa ngokuvumelana nefomula (1):
X1=(V-V0)×C×M×10-3×100
Kufomula: V - umthamo wesisombululo esijwayelekile se-cerium sulfate esisetshenziselwa ukukhishwa kwesixazululo sokuhlola, mL;
I-V0 - isixazululo esijwayelekile se-cerium sulfate esisetshenziselwa ukukhishwa kwesisombululo esingenalutho, mL;
C - Ukugxila kwangempela kwesisombululo esijwayelekile se-cerium sulfate, i-mol/L
5. Ukubalwa kokuqukethwe kwensimbi kuma-chelates
Okuqukethwe kwensimbi i-X2 ku-chelate ngokwengxenye enkulu yensimbi, inani elivezwe ku-%, libalwe ngokuvumelana nefomula: x2 = ((V1-V2) × C × 0.05585)/m1 × 100
Kufomula: I-V1 - umthamo wesisombululo esijwayelekile se-cerium sulfate esisetshenziselwa ukulinganisa kwesixazululo sokuhlola, mL;
I-V2 - isixazululo esijwayelekile se-cerium sulfate esisetshenziselwa ukukhishwa kwesixazululo esingenalutho, mL;
C - Ukuhlushwa kwangempela kwesisombululo esijwayelekile se-cerium sulfate, i-mol/L;
0.05585 - isisindo sensimbi eyinsimbi evezwa ngamagremu okulingana no-1.00 mL wesixazululo esijwayelekile se-cerium sulfate C[Ce(SO4)2.4H20] = 1.000 mol/L.
m1-Ubunzima besampula, g. Thatha isilinganiso se-arithmetic semiphumela yokunquma okufanayo njengemiphumela yokunquma, futhi umehluko ophelele wemiphumela yokunquma okufanayo awukho ngaphezu kuka-0.3%.
6. Ukubalwa kwesilinganiso se-chelation
Isilinganiso se-Chelation X3, inani elivezwe nge-%, X3 = X2/X1 × 100
I-Appendix C: Izindlela Zokunqunywa kwesilinganiso se-chelation se-Zinpro
Ukwamukelwa kwezinga: Q/320205 KAVNO7-2016
1. Ama-reagents nezinto zokwakha
a) I-glacial acetic acid: ihlanzekile ngokuhlaziya; b) I-Perchloric acid: 0.0500mol/L; c) Inkomba: 0.1% inkomba ye-crystal violet (glacial acetic acid)
2. Ukunqunywa kwama-amino acid amahhala
2.1 Amasampula omisiwe ku-80 ° C ihora elingu-1.
2.2 Beka isampula esitsheni esomile ukuze liphole ngokwezinga lokushisa elilingana negumbi noma liphole lifike ezingeni lokushisa elisebenzisekayo.
2.3 Kala cishe u-0.1 g wesampula (okunembile kuye ku-0.001 g) ube yi-250 mL eyomile yeflask eyikholi
2.4 Qhubekela ngokushesha esinyathelweni esilandelayo ukuze ugweme isampula ekumunceni umswakama we-ambient.
2.5 Faka u-25mL we-glacial acetic acid futhi uhlanganise kahle isikhathi esingeqile ku-5min.
2.6 Engeza amaconsi angu-2 esibonisi se-crystal violet.
2.7 Titrate ngo-0.0500mol/L (±0.001) isisombululo esijwayelekile se-titration se-perchloric acid kuze kube yilapho isixazululo sishintsha sisuka kokunsomi siye koluhlaza okweminyaka engu-15 ngaphandle kokushintsha umbala njengephoyinti lokugcina.
2.8 Rekhoda umthamo wesixazululo esijwayelekile esisetshenzisiwe.
2.9 Yenza isivivinyo esingenalutho ngesikhathi esifanayo.
3. Ukubalwa kanye nemiphumela
Okuqukethwe kwe-amino acid yamahhala engu-X ku-reagent kuvezwa njengengxenye enkulu (%), ibalwa ngokuvumelana nefomula (1): X=C×(V1-V0) ×0.1445/M×100%...... .......(1)
Kufomula: C - ukugxila kwesisombululo esijwayelekile se-perchloric acid kuma-moles ilitha ngalinye (i-mol/L)
I-V1 - Ivolumu esetshenziselwa ukulinganisa amasampula anesisombululo esijwayelekile se-perchloric acid, ngamamililitha (mL).
Ivolumu - Ivolumu esetshenziselwa ukusho lutho okungenalutho nesisombululo esijwayelekile se-perchloric acid, ngamamililitha (mL);
M - Isisindo sesampula, ngamagremu (g).
0.1445 - Isilinganiso sesisindo sama-amino acid esilingana no-1.00 mL wesisombululo esijwayelekile se-perchloric acid [c (HClO4) = 1.000 mol / L].
4. Ukubalwa kwesilinganiso se-chelation
Izinga le-chelation yesampula ivezwa njengengxenye enkulu (%), ibalwa ngokuvumelana nefomula (2): isilinganiso se-chelation = (ingqikithi yokuqukethwe kwe-amino acid - okuqukethwe kwamahhala kwe-amino acid)/ingqikithi yokuqukethwe kwe-amino acid×100%.
Isikhathi sokuthumela: Sep-17-2025
